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从含锑烟尘中制备纳米立方晶型Sb2O3

Keywords: 含锑烟尘,真空蒸发,纳米三氧化二锑

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Abstract:

以含锑烟尘为原料,经脱杂处理后,采用真空蒸发法制备了立方晶型纳米三氧化二锑,并用XRD衍射和SEM扫描电镜对产物三氧化二锑进行表征。结果表明,制备的三氧化二锑为立方晶型,颗粒粒径为35~100nm。实验考察了脱杂时间对脱杂效果的影响;考察了蒸发温度、压强、蒸发时间3个因素对三氧化二锑颗粒粒度的影响。

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