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色谱  2010 

Fast determination of active components in Angelica dahurica extract using capillary electrochromatography with methacrylate ester-based monolithic columns
甲基丙烯酸酯整体柱毛细管电色谱法快速分析白芷中的主要活性成分

Keywords: methacrylate ester-based monolithic column,capillary electrochromatography (CEC),imperatorin,phelloptorin,falcarindiol,isoimperatorin,Angelica dahurica
甲基丙烯酸酯整体柱
,毛细管电色谱,欧前胡素,珊瑚菜内酯,发卡二醇,异欧前胡素,白芷

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Abstract:

The separation and determination of four important active components(imperatorin,isoimperatorin,phelloptorin and falcarindiol) from Angelica dahurica extract has been performed using capillary electrochromatography(CEC) with a methacrylate ester-based monolithic column.The effect of the porogen ratio on the column preparation was studied.The mobile phase composition,such as the concentration of organic solvent,the ionic strength and the pH of the buffer were also optimized.Under the optimized conditions(50%...

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