%0 Journal Article %T Aplica£¿£¿o da espectroscopia no infravermelho e difra£¿£¿o de raio-X na determina£¿£¿o de sacarina em ado£¿antes l¨ªquidos artificiais pelo m¨¦todo volum¨¦trico com Ag+ %A Lima %A Jhonatas de Souza %A Dias %A Mauro Cesar %A Matencio %A T¨²lio %J Ecl¨¦tica Qu¨ªmica %D 2010 %I Scientific Electronic Library Online %R 10.1590/S0100-46702010000400003 %X the use of sweeteners liquid from saccharin sodium is a public health issue by the relationship with obesity and a source of sodium. the levels of saccharin were studied in four different manufacturers in samples from trade in vit¨®ria / es, between years 2006 and 2008. levels were found with values between 260 and 505 above of resolution rdc n0-8, 25/03/2008 from anvisa, which is 0,015 g/100 ml for saccharin and its salts. the profile of the crystallized sweeteners samples were evaluated by infrared spectroscopy and powder x-ray diffraction. the selectivity of the classic method of precipitation with agno3 was also verified by the techniques applied in silver saccharinate precipitates. %K sweeteners %K saccharin %K infrared %K x-ray. %U http://www.scielo.br/scielo.php?script=sci_abstract&pid=S0100-46702010000400003&lng=en&nrm=iso&tlng=en