%0 Journal Article %T A Pioneering Approach to the Synthesis of Silver Nanoparticles %A Wasan A. Al-Dulaimi %A Zeena M. Al-Azzawi %A Emad K. Al-Shakarchi %J Journal of Materials Science and Chemical Engineering %P 14-22 %@ 2327-6053 %D 2024 %I Scientific Research Publishing %R 10.4236/msce.2024.127002 %X Our research introduces a groundbreaking chemical reduction method for synthesizing silver nanoparticles, marking a significant advancement in the field. The nanoparticles were meticulously characterized using various techniques, including optical analysis, structural analysis, transmission electron microscopy (TEM), and field-emission scanning electron microscope (FESEM). This thorough process instills confidence in the accuracy of our findings. The results unveiled that the silver nanoparticles had a diameter of less than 20 nm, a finding of great importance. The absorption spectrum decreased in the peak wavelength range (405 - 394 mm) with increasing concentrations of Ag nanoparticles in the range (1 - 5%). The XRD results indicated a cubic crystal structure for silver nanoparticles with the lattice constant (a = 4.0855 Å), and Miller indices were (111), (002), (002), and (113). The simulation on the XRD pattern showed a face center cubic phase with space group Fm-3m, providing valuable insights into the structure of the nanoparticles. %K Chemical Reduction Method %K UV-VIS Absorption Spectrometer %K Field-Emission Scanning Electron Microscope (FESEM) %K Transmission Electron Microscopy (TEM) %U http://www.scirp.org/journal/PaperInformation.aspx?PaperID=134691