%0 Journal Article %T Preparation of Corncob-Like WO<sub>3</sub> Nanomaterials and Their Photocatalytic Treatment of Toluene %A Jianhai Wang %A Lu Lu %A Bing Xu %A Hongfeng Xu %A Hongwen Liu %J Journal of Materials Science and Chemical Engineering %P 84-93 %@ 2327-6053 %D 2024 %I Scientific Research Publishing %R 10.4236/msce.2024.122007 %X Corn rod-like WO3 nanomaterials were successfully synthesized by a simple hydrothermal method. The morphology, structure and optical absorption properties of the prepared samples were characterized by SEM, XRD, FTIR and UV-Vis-DRS. The WO3 materials were corn rod-like morphology with about 800 nm for length and 150 nm for diameter, especially there were plenty of corn particles (about 20 nm) on the surface of corn rods. The X-ray diffraction peaks of the products corresponded with WO3 standard card, and the characteristic peak of W-O bond was found in the infrared spectrum. The absorption band edge of the products was about 480 nm, indicating their potential visible-light-induced photocatalytic activity. In situ FTIR technology research showed that the prepared WO3 nanomaterials had visible photocatalytic activity to gas-phase toluene. After a photocatalytic reaction for 8 hours toluene was effectively degraded, and carboxylic acid and aldehyde could be regarded as the intermediate products, and CO2 was produced as the final product during the reaction process. %K WO< %K sub> %K 3< %K /sub> %K Nanomaterials %K Visiblelight %K Photocatalytic Degradation %K Toluene %K < %K i> %K In Situ< %K /i> %K FTIR %U http://www.scirp.org/journal/PaperInformation.aspx?PaperID=131452