%0 Journal Article %T Temperature-Program Assisted Synthesis of Novel Z-Scheme CuBi2O4/¦Â-Bi2O3 Composite with Enhanced Visible Light Photocatalytic Performance %A Chunmo Yu %A Ning Li %A Runliang Zhu %A Shuai Li %A Song Xu %A Wei Xia %A Xiaojuan Chen %A Xin Chen %J Archive of "Nanomaterials". %D 2018 %R 10.3390/nano8080579 %X Novel Z-Scheme CuBi2O4/¦Â-Bi2O3 composite photocatalysts with different mass ratios and calcination temperatures were firstly synthesized by the hydrothermal method following a temperature-programmed process. The morphology, crystal structure, and light absorption properties of the as-prepared samples were systematically characterized, and the composites exhibited enhanced photocatalytic activity toward diclofenac sodium (DS) degradation compared with CuBi2O4 and ¦Â-Bi2O3 under visible light irradiation. The optimal photocatalytic efficiency of the composite, achieved at the mass ratio of CuBi2O4 and ¦Â-Bi2O3 of 1:2.25 and the calcination temperature of 600 ¡ãC is 92.17%. After the seventh recycling of the composite, the degradation of DS can still reach 82.95%. The enhanced photocatalytic activity of CuBi2O4/¦Â-Bi2O3 is closely related to OH£¿, h+ and O2£¿£¿, and the photocatalytic mechanism of CuBi2O4/¦Â-Bi2O3 can be explained by the Z-Scheme theory %K CuBi2O4/¦Â-Bi2O3 %K temperature programmed %K semiconductors %K Z-Scheme %K visible light %K organics %U https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6116239/