%0 Journal Article %T 磁性纳米氧化铝球的合成及性能研究
Preparation and Character Investigation of Magnetic Alumina Nanospheres %A 刘澄虎 %A 刘晓月 %A 庞茂森 %A 冯志浩 %A 苗长青 %A 付庆涛 %J Hans Journal of Chemical Engineering and Technology %P 153-159 %@ 2161-8852 %D 2019 %I Hans Publishing %R 10.12677/HJCET.2019.93022 %X 本文以α-α-Fe2O3核,硬脂酸为模板剂,通过异丙醇铝水解,缩聚过程以及模板剂自组装合成了一种新型均一核壳结构氧化铁/氧化铝纳米球,然后通过H2/N2还原得到磁性氧化铝球。该纳米球具有均一壳层,厚度为30 nm,比表面积为140 m2/g,孔容为0.22 cm3/g,比饱和磁化强度为50.2 emu/g。
Well-structured nanospheres with a magnetic core/alumina shell (MFeCA) structure were obtained by self-assembly of stearic acid/alumina species complex in 1-propanol system. The thickness of alumina uniform shell is around 30 nm. The surface area, pore volume and average pore size of the sample are 140 m2/g, 0.22 cm3/g and 5.2 nm, respectively. The saturation magnetization values of the sample are as high as 50.2 emu/g.
%K α-氧化铁,溶胶–凝胶法,自组装,磁性氧化铝纳米球
α-Fe2O3 %K Sol-Gel Method %K Self-Assembly %K Magnetic Nanospheres %U http://www.hanspub.org/journal/PaperInformation.aspx?PaperID=29723