%0 Journal Article
%T 天台乌药挥发油成分的提取及气质联用分析<br>Extraction and GC-MS Analysis of Volatile Oil from Lindera aggregata (Sims) Kosterm
%A 叶婧
%A 赵琳
%A 卢延斌
%A 张虹
%J Advances in Analytical Chemistry
%P 186-193
%@ 2163-1565
%D 2019
%I Hans Publishing
%R 10.12677/AAC.2019.93025
%X <div style=\"text-align:justify;\">
	本文以浙江省特色中药材天台乌药为原料，采用水蒸气蒸馏法提取其中的挥发油成分。分别考察了浸泡时间、提取时间、料液比对挥发油提取效率的影响，实验结果表明天台乌药挥发油成分的最佳提取条件为：浸泡时间3 h、提取时间3 h、料液比为1:12。在此条件下，天台乌药挥发油的提取率约为0.36%。采用GC-MS法分析天台乌药挥发油的化学成分。经过标准谱库检索并与相关文献进行比对，共鉴定出了39个化学成分，其中大多数为萜类化合物。<br />
The volatile oil of Lindera aggregata (Sims) Kosterm was extracted by traditional distillation method. The effects of soaking time, extraction time and liquid-material ratio on the extraction ef-ficiency of volatile oil were investigated. The results showed that the optimum extraction conditions were as follows: the soaking time of 3 hours, the extraction time of 3 hours and the ratio of liquid to material of 12:1. Under the optimum conditions, the extraction yield of 0.36% was obtained. The volatile oil extracted was analyzed by GC-MS to determine the chemical constituents of volatile oil in Lindera aggregata (Sims) Kosterm. The results indicated that totally 39 compounds were identified compared with the GC-MS database and most of them were terpenoids.
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%K 天台乌药，挥发油，提取，气相色谱–质谱法(GC-MS)<br>Lindera aggregata (Sims) Kosterm
%K Volatile Oil
%K Extraction
%K Gas Chromatography-Mass Spectrometry (GC-MS)
%U http://www.hanspub.org/journal/PaperInformation.aspx?PaperID=31865