%0 Journal Article %T Photoluminescence Emission Control of Porous Silicon %A Marwa Nabil %J Soft Nanoscience Letters %P 35-44 %@ 2160-0740 %D 2019 %I Scientific Research Publishing %R 10.4236/snl.2019.93003 %X This paper reports the feasibility of synthesis and characterization of nano-porous silicon (NPS) powder and (Nickel/nano-porous silicon, Ni/NPS) nano-composite prepared using dual techniques (alkaline chemical etching process and ultra-sonication technique). The structural and the optical properties of the fabricated structures are inspected using X-ray Diffraction, Fourier Transform Infrared Spectrophotometer, Raman Spec-troscopy, and Fluorescence Spectrophotometer Photoluminescence. All the results have agreed that NPS is one of the most suitable materials used as active material in the LED fabrication; by changing the main factors in the preparation process, so the different physical and chemical properties are obtained. NPS produces two emission regions that correspond to orange-red and dark red; on the other hand, (Ni/NPS) produce the yellow emission. So, the photoluminescence emission is controllable by adjusting the preparation conditions. The optical data recorded here are useful for the production of the nanoscale optical devices. %K Optical Materials %K Chemical Synthesis %K Optical Properties %U http://www.scirp.org/journal/PaperInformation.aspx?PaperID=95929