%0 Journal Article %T ZnO纳米线与硫掺杂TiO2微/纳复合材料的制备及其光催化活性<br>Study on preparation and photocatalytic activity of micro/nano-structured ZnO/ S-doped TiO2 composite %A 张延霖 谢楚如 蔡文娟 吴宏海 %J 华南师范大学学报(自然科学版) %D 2016 %R 10.6054/j.jscnun.2015.08.021 %X 采用水热法制备了ZnO纳米线与硫掺杂TiO2(ZnO/S-TiO2)微/纳复合光催化剂,通过SEM、XRD、XPS对复合光催化剂进行表征,探讨了硫掺杂量和煅烧温度对该复合催化剂光催化性能的影响。结果表明,ZnO微米线表面形成了粒径较为均一的纳米S-TiO2颗粒,硫掺杂TiO2中形成了Ti-O-S键;当硫掺杂量为0.8mol%并经500℃高温煅烧的复合光催化剂对菲的降解呈现出最好的光催化活性。<br>: Micro/nano-structured ZnO/S-doped TiO2 composite (ZnO/S-TiO2) has been successfully prepared by hydrothermal method. The structure and morphology of the ZnO/S-TiO2 composite were characterized by SEM, XRD and XPS. The effect of dosage of sulfur doping into titanium dioxide and calcination temperature on photocatalytic activity of ZnO/S-TiO2 composite was discussed. The result indicated that Ti-O-S bond existed and homogeneous S doped TiO2 nanoparticles could be formed on the surface of ZnO. Under the conditions of 0.8 mol% of sulfur doping and the calcination temperature of 500℃, the synthesized photocatalyst exhibited the best photocatalytic activity for degradation of phenanthrene %U http://journal.scnu.edu.cn:8080/jwk_xbzrb/CN/abstract/abstract3660.shtml