%0 Journal Article
%T Synthesis of High-Thermal Stable Titanium Dioxide Nanoparticles
%A M. Rashidzadeh
%J International Journal of Photoenergy
%D 2008
%I Hindawi Publishing Corporation
%R 10.1155/2008/245981
%X Nanosized crystals of anatase phase TiO2 with high-thermal stability was synthesized in the range of 15–17 nm via sol-gel method using titanium n-butoxide precursor. Synthesize was done at two different temperatures, that is, 200 and 300ˇăC and the final products were calcined at 400ˇăC. The final products were characterized by N2 adsorption, X-ray diffraction, FT-IR, and TEM and tested in a photoreactor using fluorescien as model molecule. For thermal stability investigation, the sample prepared at 300ˇăC was heated up to 800, 850, and 900ˇăC, the XRD results showed that the synthesized anatase phase was stable up to 850ˇăC. Photocatalytic activity of the prepared samples showed that the fluorescien degradation followed a pseudo-first-order kinetic.
%U http://www.hindawi.com/journals/ijp/2008/245981/