%0 Journal Article
%T Crystal structure of N,N,N',N'-tetramethylethylenediammonium dinitrate
%A Zaouali Zgolli Donia
%A Hbib Boughzala
%A Ahmed Driss
%J European Journal of Chemistry
%D 2011
%I 
%R 10.5155/eurjchem.2.3.314-316.307
%X N,N,N',N'-tetramethylethylenediammonium dinitrate has been synthesized. The crystal and molecular structure of the title compound has been determined from single crystal X-ray diffraction data. C6H18N4O6, M =242.24, Triclinic, a = 6.040(2)  , b = 6.834(3)  , c = 7.867(2)  , ¦Á = 74.1120(10)¡ã, ¦Â = 83.700(2)¡ã, ¦Ã = 80.314(2)¡ã, V = 307.12(19)  3, T = 298(2) K, space group P-1 (no. 2), Z = 1, ¦Ì(Mo-K¦Á) = 0.115, 2383 reflections measured, 1342 unique (Rint = 0.0169) which were used in all calculations. The final wR(F2) was 0.1262 (all data). In the title compound, C6H18N22+.2NO3-, both N atoms of the cationic moiety are protonated and linked via hydrogen bonds to two trigonal planar nitrate anions. Two types of classical hydrogen bonds are observed: N1-H¡­O1 and N1-H¡­O2. These bonds link the cations and the anions together, forming a one-dimensional network and reinforcing the cohesion of the ionic structure.
%K N
%K N
%K N'
%K N'-tetramethylethylenediammonium dinitrate
%K Single crystal structure
%K Organic-inorganic
%K Synthesis
%K Characterization
%K Hydrogen©\bond
%U http://www.eurjchem.com/index.php/eurjchem/article/view/307