%0 Journal Article
%T Synthesis, characterization and crystal structure of 1-(4-methylbenzoyl)-3-(4 aminosulfonylphenyl)thiourea
%A Aamer Saeed
%A Amara Mumtaz
%A Ulrich Florke
%J European Journal of Chemistry
%D 2010
%I 
%R 10.5155/eurjchem.1.2.73-75.34
%X An efficient synthesis of the title compound, 1-(4-methylbenzoyl)-3-(4-aminosulfonyl phenyl)thiourea,  was carried out by reaction of 4-methylbenzoyl chloride with potassium thiocyanate in acetone to afford 4-methylbenzoyl isothiocyanate in situ followed by treatment with sulfanilamide. The structure was confirmed by spectroscopic data and elemental analyses. The molecular structure was determined from single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P21/n with unit cell dimensions of a = 4.8116(9)  , b = 17.150(3)  , c = 18.677(3)  , ¦Ã = 96.487(4) ¡ã, and V = 1531.4(5)  3.
%K Thiourea
%K Sulfonyl thiourea
%K Single crystal X-ray diffraction
%U http://www.eurjchem.com/index.php/eurjchem/article/view/34