%0 Journal Article
%T PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION
%A BAHRAM MOKHTARI
%A KOBRA POURABDOLLAH
%J Journal of the Chilean Chemical Society
%D 2012
%I Sociedad Chilena de Qu¨ªmica
%X A new sensitive method for determination of salbutamol, as a nutrient repartitioning agent, in livestock is presented to protect the consumers. Eight nano-baskets of p-tert-calix[4]arene bearing di-[N-(X)sulfonyl carboxamide] and di-(1-propoxy) in partial-cone conformation were synthesized and were used to prepare bended phases of HPLC-UV. The new synthesized bonded-phases were characterized and optimized, the bonding interactions of solute and stationary phases were examined and the main interactions were reported. The results revealed that for the best bonded-phase, the LOD and LOQ were 0.02 and 0.06 ¦̀g/mL, respectively.
%K Bonded-Phase
%K Partial-Cone Conformation
%K Calixarene
%K Salbutamol
%K nanobasket
%U http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000200020