%0 Journal Article %T Sonochemicial Synthesis of AgSbTe2 Thermoelectric Compounds %A XU Jing-Jing %A DU Bao-Li %A ZHANG Wen-Hao %A TANG Xin-Feng %J 无机材料学报 %D 2010 %I Science Press %R 10.3724/sp.j.1077.2010.00593 %X Single-phase AgSbTe2 powder was synthesized by sonochemicial method combining with deoxidizing heat-treatment. The influences of heat-treatment temperature, time and the initial ratio of starting reactants on the phases of the final products were investigated. Near single-phase AgSbTe2 ternary powder can be obtained after 2h heat treatment under 500 Degrees, and single-phase AgSbTe2 can be obtained by changing the initio ratio of the starting reactants. Microstructure analysis shows that nanodots with dimension of 20-50nm are uniformly distributed on the surface of the as-prepared powders with the average size of about 10m. A dimensionless thermoelectric figure of merit ZT = 1.14 is obtained at 570K for the sample with single phase. %K AgSbTe2 %K sonochemicial method %K heat treament %K thermoelectric materials %U http://www.jim.org.cn/fileup/PDF/20100607.pdf