%0 Journal Article
%T Benzyl 3-deoxy-3-(3,4,5-trimethoxybenzylamino)-¦Â-L-xylopyranoside
%A Fulgentius Nelson Lugemwa
%J Molbank
%D 2013
%I MDPI AG
%R 10.3390/M793
%X Reaction of 3,4,5-trimethoxybenzylamine and benzyl 2,3-anhydro-¦Â-L-ribopyranoside in refluxing ethanol produced benzyl 3-deoxy-3-(3,4,5-trimethoxybenzylamino)-¦Â-L-xylopyranoside in 72.5% yield. An attempt to synthesize the title compound by reacting neat 3,4,5-trimethoxybenzylamine with benzyl 2,3-anhydro-¦Â-L-ribopyranoside without a solvent produced a dark brown mixture with several decomposition products. The structure of benzyl 3-deoxy-3-(3,4,5-trimethoxybenzylamino)-¦Â-L-xylopyranoside was determined using elemental analysis, 1H-NMR and 13C-NMR and its conformation is 1 C 4 .
%K epoxide ring-opening
%K 3
%K 4
%K 5-trimethoxybenzylamine
%K benzyl 2
%K 3-anhydro-¦Â-L-ribopyranoside
%U http://www.mdpi.com/1422-8599/2013/1/M793