%0 Journal Article
%T MICROWAVE-ASSISTED SYNTHESIS OF 2-SUBSTITUTED-4H-3, 1-BENZOXAZIN- 4-ONES IN TETRAETHYLAMMONIUM CHLORIDE AS AN IONIC LIQUID Mikrowellen-unterst¨¹tzte Synthese von 2-substituierten-4H-3, 1-benzoxazin- 4-ONES IN Tetraethylammoniumchlorid als ionische Fl¨¹ssigkeit
%A Ali Dorehgiraee
%A Hojatollah Khabazzadeh and Kazem Saidi
%J Heterocyclic Letters
%D 2012
%I Raman Publications
%R july 25, 2012.
%X A series of 2-substituted 4H-3, 1-benzoxazine-4-ones were synthesized from N-acyl anthranilic acid in the presence molten tetraethylammonium chloride as an ionic liquid under microwave irradiation. The advantages of this procedure is the employment of Mg(HSO4)2, a dehydrating agent as a catalyst instead of acetic anhydride, shorter reaction time, easy workup and high yield of the products.
%K benzoxazine-4-one
%K ionic liquid
%K microwave
%K tetraethyl ammonium chloride
%U http://heteroletters.org/issue24/2.html