%0 Journal Article
%T Analysis of Phenolic Compounds in Mineral Water by High Performance Liquid Chromatography(HPLC)
高效液相色谱法分析矿泉水中酚类化合物
%A X Zhang
%A R Wu
%A
张学俊
%A 吴仁安
%J 色谱
%D 1998
%I
%X A high performance liquid chromatographic method for the simultaneous analysis of phenolic compounds, such as, phenol, m-cresol, bisphenol A, bisphenol F, 4-tert-butylphenol, bisphenol F diglycidyl ether (BFDGE) and bisphenol A diglycidyl ether (BADGE) in mineral water with fluorometric detector is described in this paper. After pretreatment through solid-liquid extraction, the sample was analyzed by HPLC. The operating conditions were Turner C18, 5 microns, column, 150 mm x 4.6 mm i.d., mobile phase with V(ACN): V(water) = 40:60 for 10 min, then linear gradient elution for 25 min up to 80:20 with a flow rate of 1.3 mL/min. Excitation wavelength was set at 275 nm and emmission at 300 nm. The recoveries were 81%-105% and the RSDs were 1.12%-13.21%. Detection limit reached 0.1-0.2 microgram/L.
%K high performance liquid chromatography
%K analysis of mineral water
%K phenolic compounds
矿泉水分析
%K 酚类
%K HPLC
%K 饮料
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=F65B1163FA62F63D8719A1D383FDF09B&yid=8CAA3A429E3EA654&vid=7801E6FC5AE9020C&iid=B31275AF3241DB2D&sid=BB98BB04E861B6F5&eid=20ADD38F841C6A4B&journal_id=1000-8713&journal_name=色谱&referenced_num=22&reference_num=1