%0 Journal Article %T Chiral Separation of 3-Phenyllactic Acid by Capillary Electrophoresis
3-苯基乳酸的手性毛细管电泳拆分 %A LI Demao %A LI Congfa %A LIU Sixin %A CHEN Limei %A
李德茂 %A 李从发 %A 刘四新 %A 陈利梅 %J 色谱 %D 2004 %I %X Various factors affecting the chiral resolution of 3-phenyllactic acid by capillary zone electrophoresis such as the type of cyclodextrin, concentration of the chiral selector, buffer pH, voltage, and temperature were studied and optimized. Using 30 mmol/L hydroxypropyl-beta-cyclodextrin as the chiral selector, and 0.1 mol/L phosphate solution (pH 5.5) as the running buffer, the baseline separation of 3-phenyllactic acid enantiomers was achieved with a resolution factor of 1.51. The separation voltage was 26 kV and the temperature was 25 degrees C. %K NULL
毛细管电泳 %K 3-苯基乳酸 %K 羟丙基-β-环糊精 %K 手性分离 %U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=AF8D1426462BEABA&yid=D0E58B75BFD8E51C&vid=BC12EA701C895178&iid=38B194292C032A66&sid=C1B34927D429E92F&eid=E2B9962CCD971A0D&journal_id=1000-8713&journal_name=色谱&referenced_num=5&reference_num=14