%0 Journal Article %T Determination of Brucine in Seed Dressing Agents by High Performance Liquid Chromatography
高效液相色谱法测定农药拌种剂中的马钱子碱 %A ZHU Zhi-jia %A
朱智甲 %J 色谱 %D 2000 %I %X An HPLC method for the determination of brucine in seed dressing agents was investigated. The sample solution was separated on a Spherisorb C18 column(4.6 mm i.d. x 200 mm, 5 microns) with CH3OH-H2O-CTAB (88:12:0.04, m/m) as the mobile phase and detected at 254 nm. Calibration curve of brucine was obtained for the concentration range of 0.01 g/L-0.25 g/L. The linear regression equation was A = 11,485,814 rho + 21,229, r = 0.9997. The RSD was 1.2%(n = 11). The results show that this method is simple, specific and accurate. %K high performance liquid chromatography %K seed dressing sample %K brucine
高效液相色谱法 %K 农药拌种剂 %K 马钱子碱 %K 分析 %U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=17E0DC901637367E&yid=9806D0D4EAA9BED3&vid=13553B2D12F347E8&iid=94C357A881DFC066&sid=3FC4D669D19FF0C6&eid=8F2250DA83AF77B8&journal_id=1000-8713&journal_name=色谱&referenced_num=0&reference_num=0