%0 Journal Article
%T The Synthesis of Phenyl-Silica Gel and Its Application in Purification of Taxol<br>苯基-硅胶色谱介质的合成及其在紫杉醇提纯中的应用
%A TIAN Gui lian
%A ZHANG Zhi qiang
%A SU Zhi guo
%A <br>田桂莲
%A 张志强
%A 苏志国
%J 色谱
%D 2001
%I 
%X Phenyl-silica gels were synthesized with four methods of reaction on gamma-aminopropyltriethoxysilane (APTS) silica gel. The synthesized gels were used as stationary phase of normal pressure chromatography to separate and purify taxol. The comparison of these four silica gels was carried out. It was found that the gel synthesized by gas-phase reaction gave the best results. The purity of taxol was 77.4%, and the recovery was about 90%.
%K NULL<br>硅胶
%K γ－氨丙基三乙氧基硅烷
%K 苯基－硅胶
%K 紫杉醇
%K 反相液相色谱
%K 提纯
%K 色谱介质
%K 分离
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=EBBB89F9054DA486&yid=14E7EF987E4155E6&vid=2A8D03AD8076A2E3&iid=CA4FD0336C81A37A&sid=F4B561950EE1D31A&eid=771152D1ADC1C0EB&journal_id=1000-8713&journal_name=色谱&referenced_num=3&reference_num=5