%0 Journal Article
%T Determination of Inorganic Anions in Herba Ephedrae by Ion Chromatography
离子色谱法测定麻黄中的无机阴离子
%A FU Jihong
%A XIE Chengxi
%A ZHANG Lijing
%A
符继红
%A 解成喜
%A 张丽静
%J 色谱
%D 2004
%I
%X An ion chromatographic method for the detemination of inorganic anions in Herba Ephedrae was developed. The separation of the anions was achieved on a Shim-Pack IC-AI column with a mixture of 2.5mmol/L phthalic acid and 2.4mmol/L tris(hydroxymethyl)amino-methane as mobile phase, and the detection was performed by a conductivity detector. Fluori-de, chloride, nitrite, bromide, nitrate and sulfate could be identified within 10 min.The method is simple and useful, and has good linearity with correlation coefficients between 0.999 2 and 0.999 7 and relative standard deviations lower than 1.92%. The recoveries of anions in the samples were between 96.6% and 100.4%.
%K ion chromatography
%K inorganic anion
%K Herba Ephedrae
药用植物
%K 麻黄
%K 无机阴离子
%K 测定
%K 离子色谱法
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=632C9599D5A54125&yid=D0E58B75BFD8E51C&vid=BC12EA701C895178&iid=CA4FD0336C81A37A&sid=AA76E167F386B6B3&eid=B9704B40A4225A24&journal_id=1000-8713&journal_name=色谱&referenced_num=10&reference_num=3