%0 Journal Article %T Determination of Inorganic Anions in Herba Ephedrae by Ion Chromatography
离子色谱法测定麻黄中的无机阴离子 %A FU Jihong %A XIE Chengxi %A ZHANG Lijing %A
符继红 %A 解成喜 %A 张丽静 %J 色谱 %D 2004 %I %X An ion chromatographic method for the detemination of inorganic anions in Herba Ephedrae was developed. The separation of the anions was achieved on a Shim-Pack IC-AI column with a mixture of 2.5mmol/L phthalic acid and 2.4mmol/L tris(hydroxymethyl)amino-methane as mobile phase, and the detection was performed by a conductivity detector. Fluori-de, chloride, nitrite, bromide, nitrate and sulfate could be identified within 10 min.The method is simple and useful, and has good linearity with correlation coefficients between 0.999 2 and 0.999 7 and relative standard deviations lower than 1.92%. The recoveries of anions in the samples were between 96.6% and 100.4%. %K ion chromatography %K inorganic anion %K Herba Ephedrae
药用植物 %K 麻黄 %K 无机阴离子 %K 测定 %K 离子色谱法 %U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=632C9599D5A54125&yid=D0E58B75BFD8E51C&vid=BC12EA701C895178&iid=CA4FD0336C81A37A&sid=AA76E167F386B6B3&eid=B9704B40A4225A24&journal_id=1000-8713&journal_name=色谱&referenced_num=10&reference_num=3