%0 Journal Article
%T Determination of alkylphenols and alkylphenol polyethoxylates in textiles by normal-phase high performance liquid chromatography and solid-phase extraction<br>固相萃取净化-正相高效液相色谱测定纺织品中残留的烷基酚和烷基酚聚氧乙烯醚
%A L Chunhua
%A CHEN Xiaomei
%A LIU Haishan
%A <br>吕春华
%A 陈笑梅
%A 刘海山
%J 色谱
%D 2009
%I 
%X 建立了测定纺织品中烷基酚(AP)和烷基酚聚氧乙烯醚(APnEO)(n2～16)的正相高效液相色谱法。以甲醇为提取溶剂,用索氏抽提法提取纺织品中的AP和APnEO,用正相高效液相色谱法测定,并对提取溶剂、提取方式和净化条件等前处理条件进行优化。该方法的检出限为1.0 mg/kg,回收率为90.4%～104.1%,相对标准偏差为0.64%～4.21%。采用该方法对多种基质纺织品进行检测,可满足残留检测要求。
%K normal-phase high performance liquid chromatography (NP-HPLC)
%K alkylphenols
%K alkylphenol polyethoxylates
%K textiles<br>正相高效液相色谱法
%K 烷基酚
%K 烷基酚聚氧乙烯醚
%K 纺织品
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=B03C836CC0523F8C24C34A1F35EB0E66&yid=DE12191FBD62783C&vid=DB817633AA4F79B9&iid=E158A972A605785F&sid=D9202C57BAB9096F&eid=8C5DE51F0A009A0F&journal_id=1000-8713&journal_name=色谱&referenced_num=0&reference_num=13