%0 Journal Article
%T Effect of the Bonding Amounts of Chiral Ligand Exchange Chromatogr-aphic Stationary Phases on the Enantioseparation of Amino Acids<br>硅胶键合手性配体交换固定相键合量对α-氨基酸拆分的影响
%A ZHU Xin yi
%A HAN Xiao qian
%A QI Bang feng
%A LI Yong min
%A JIANG Sheng xiang
%A CHEN Li ren
%A <br>祝馨怡
%A 韩小茜
%A 齐邦峰
%A 李永民
%A 蒋生祥
%A 陈立仁
%J 色谱
%D 2002
%I 
%X L proline chiral stationary phases with various bonding amounts for ligand exchange chromatography were prepared by treating silica gel with 3 glycidoxypropyltrimethoxysilane and bonding L proline. The bonding amounts of L proline chiral stationary phase were controlled effectively and characterized by IR and elemental analysis. Some DL amino acids were separated and the influences of the bonding amounts on the efficiency of resolution of DL amino acids by ligand exchange chromatography were briefly discussed and explained by the mechanism of the separation.
%K 硅胶键合手性配体
%K 配体交换色谱
%K L－脯氨酸
%K 手性固定相
%K 对映体分离
%K 键合量
%K α－氨基酸
%K 手性拆分
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=99D69BC7900359CF&yid=C3ACC247184A22C1&vid=A04140E723CB732E&iid=38B194292C032A66&sid=E089FDF3CDAE8561&eid=6ED15D8DCB279BC4&journal_id=1000-8713&journal_name=色谱&referenced_num=8&reference_num=10