%0 Journal Article %T Simultaneous Determination of Various Food Additives by High Performance Liquid Chromatography
高效液相色谱法同时测定多种食品添加剂 %A CHEN Qing chuan %A YU Wen lian %A WANG Jing %A
陈青川 %A 于文莲 %A 王静 %J 色谱 %D 2001 %I %X A novel method is proposed for the simultaneous separation and determination of eight food additives, acesulfame potassium (AK), aspartame (ASP), benzoic acid (BA), caffeine (CA), saccharin sodium (SA), sorbic acid (SOR), theobromine (TB) and theophylline (TP) by reversed-phase high performance liquid chromatography. The separation was achieved within 23 min by using an Alltech Econosphere C18 column with 10 mmol/L NaH2PO4(pH 4.00)-acetonitrile (90:10, V/V) as mobile phase. The qualification and quantitation were accomplished by using a photodiode array detector. The detection limits (S/N = 3) for all analytes were below mg/L level. Under the experimental conditions, other common food additives and organic acids such as cyclamate, citric acid, malic acid, tartaric acid and ascorbic acid, did not interfere with the determination. The method has been successfully applied to the analysis of various foods as well as pharmaceutical preparation, and the average recoveries for real samples ranged from 78.5% to 107.2%. %K high performance liquid chromatography %K food additive %K synthetic sweetener %K preservative %K caffeine %K theobromine %K theophylline
高效液相色谱法 %K 食品添加剂 %K 人工合成甜味剂 %K 防腐剂 %K 咖啡因 %K 可可碱 %K 茶碱 %K 同时测定 %U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=0E64E4D3D3450134&yid=14E7EF987E4155E6&vid=2A8D03AD8076A2E3&iid=0B39A22176CE99FB&sid=03F1579EF92A5A32&eid=6270DC1B5693DDAF&journal_id=1000-8713&journal_name=色谱&referenced_num=31&reference_num=16