%0 Journal Article
%T Determination of Swainsonine in A.variabilis Bunge by Gas Chromatography with Methyl-α-D-Mannopyranoside Internal Standard Method<br>气相色谱-甲基化-α-D-甘露糖苷内标法测定变异黄芪中的苦马豆素
%A ZHAO Xinghua
%A CUI Zhonghua
%A GENG Guoxia
%A WANG Jianhua
%A ZHANG Zhimin
%A SONG Yumin
%A LIU Zhibin
%A <br>赵兴华
%A 崔忠华
%A 耿果霞
%A 王建华
%A 张志敏
%A 宋毓民
%A 刘志滨
%J 色谱
%D 2007
%I 
%X 建立以甲基化-α-D-甘露糖苷为内标物,用气相色谱测定变异黄芪中苦马豆素的方法。植物样品经甲醇超声提取、氯仿去除杂质后,将碱性正丁醇萃取物用硅烷化试剂进行衍生化,通过AT.SE-54毛细管柱分离,氢火焰离子化检测器检测,测得变异黄芪干草粉中苦马豆素含量为115.7mg/kg,加标回收率为82.6%～94.0%,相对标准偏差为2.8%。该方法能用于疯草样品中苦马豆素的含量检测。
%K 气相色谱(GC)
%K 疯草(locoweed)
%K 苦马豆素(swainsonine)
%K 衍生化(derivatization)
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=12D738FB45E2954D&yid=A732AF04DDA03BB3&vid=C5154311167311FE&iid=94C357A881DFC066&sid=DBEE434FCBFED297&eid=B75DC817262E20A8&journal_id=1000-8713&journal_name=色谱&referenced_num=6&reference_num=6