%0 Journal Article
%T Preparation, Characterization and Evaluation of Cellulose Tris (3,5-dimethylphencarbamate) Chiral Stationary Phase<br>纤维素-三(3,5-二甲基苯基氨基甲酸酯)涂敷手性固定相的制备、表征及评价
%A HOU Jing-guo
%A DENG Qi-liang
%A MENG Xiao-rong
%A LIU Hui-ling
%A YANG Wu
%A MO Zun-li
%A GAO Jin-zhang
%A <br>侯经国
%A 邓启良
%A 孟晓蓉
%A 刘慧玲
%A 杨武
%A 莫尊理
%A 高锦章
%J 色谱
%D 2001
%I 
%X With the deposition of cellulose tris(3,5-dimethylphenylcarbamate) (CDMPC) on aminopropylated silica gel (mean particle size, 5 microns; pore size, 13 nm; surface area, 110 m2/g) by using two different methods (evaporation and precipitation), two chiral stationary phases (CSP1 and CSP2) characterized by elemental analysis and scanning electron micrography were obtained. They were also evaluated by using seven racemic compounds with n-hexane/ethanol(95/5, V/V) and n-hexane/2-propanol (90/10, V/V) as mobile phases. The results showed that the chiral stationary phase CSP1 obtained by the evaporation method had better efficiency and chiral resolution ability than CSP2 by the precipitation method.
%K high performance liquid chromatography
%K cellulose
%K tris(3
%K 5
%K dimethylphenylcarbamate)
%K chiral stationary phase<br>高效液相色谱法
%K 纤维素－三（3
%K 5－二甲基苯基氨基甲酸酯）
%K 手性固定相
%K 制备
%K 表征
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=DD04D9AF4937A577&yid=14E7EF987E4155E6&vid=2A8D03AD8076A2E3&iid=0B39A22176CE99FB&sid=E2546871E5B846EF&eid=3F0AF5EDBC960DB0&journal_id=1000-8713&journal_name=色谱&referenced_num=3&reference_num=6