%0 Journal Article %T Determination of Hesperidin and Naringin in Fructus Aurantii Immaturus and Fructus Aurantii by Reversed-Phase High Performance Liquid Chromatography
反相高效液相法测定枳实、枳壳中橙皮甙和柚皮甙的含量 %A Xiu-ling Li %A Long Li %A Hong-bin Xiao %A Xin-miao Liang %A
李秀玲 %A 李龙 %A 肖红斌 %A 梁鑫淼 %J 色谱 %D 2002 %I %X An HPLC method was established for the determination of hesperidin and naringin in the Fructus Aurantii Immaturus and Fructus Aurantii from different places. Hesperidin and narigin were separated on a Hypersil ODS1 column with acetonitrile-0.5% acetic acid (volume ratio of 22:78) as the mobile phase and detected at 283 nm. The flow rate was 1.0 mL/min. The column temperature was set at 35 degrees C. The calibration curves were linear in the ranges of 0.060 g/L-0.604 g/L and 0.0125 g/L-0.125 g/L for naringin and hesperidin respectively. The average recoveries were 97.1% for naringin and 95.3% for hesperidin. The method is simple, rapid, accurate and reliable. %K high performance liquid chromatography %K hesperidin %K naringin %K Fructus Aurantii Immaturus %K Fructus Aurantii
反相高效液相色谱法 %K 测定 %K 橙波甙 %K 柚皮甙 %K 枳实 %K 枳壳 %K 植物药 %K 分析 %U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=81698D58546FF439&yid=C3ACC247184A22C1&vid=A04140E723CB732E&iid=B31275AF3241DB2D&sid=E513158F1BE1471F&eid=CD26609C367AC9C8&journal_id=1000-8713&journal_name=色谱&referenced_num=23&reference_num=4