%0 Journal Article
%T Isolation , Purification and Identification of 2-Hydroxy-3-Butenylglucosinolate and 3-Butenylglucosinolate from Rapeseed<br>用液相制备色谱从菜籽中分离、纯化制备硫代葡萄糖苷
%A Wu Moucheng
%A Kuang Chengchen
%A and Huang Wei
%A <br>吴谋成
%A 况成尘
%A 黄伟
%J 色谱
%D 1995
%I 
%X 从我国甘蓝型、芥菜型油菜籽中，用弱离子交换剂ＤＥＡＥ Ｓｅｐｈａｄｅｘ Ａ－２５作固定相，Ｋ２ＳＯ４作流动相，采用自动柱色谱仪分离制备非吲哚类硫代葡萄糖苷结晶粗品。从非吲哚类硫代葡萄糖苷结晶粗品中进一步分离和纯化，制得２－羟基－３－丁烯基硫代葡萄糖苷的钾盐晶体，经元素，熔点分析和质谱、红外图谱，紫外图谱，紫外图谱、ＨＰＬＣ图谱证实，结晶物可作为硫代葡萄糖苷定性和定量分析时的标准物。
%K igh performance liquid chromatography
%K preparative chromatography
%K 2-hydroxy-3-butenylglucosinolate
%K 3-butenylglacosinolate
%K rapeseed<br>高效液相色谱
%K 硫代葡萄糖苷
%K 油菜籽
%K 制备
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=6579068328FE643F&jid=4D81E042D77AFEC6881D14759692069C&aid=2BD31EED9264A15946678126C9356132&yid=BBCD5003575B2B5F&vid=FC0714F8D2EB605D&iid=CA4FD0336C81A37A&sid=E158A972A605785F&eid=DF92D298D3FF1E6E&journal_id=1000-8713&journal_name=色谱&referenced_num=7&reference_num=3