%0 Journal Article %T Synthesis of 2,6-bis(benzylidene)cyclohexanone and study of liquid crystal Behavior
2,6-二亚苄基环己酮液晶化合物的合成及性能研究 %A WEI XiLian %A FU ShiZhou %A WANG DaQi %A SUN DeZhi %A YIN BaoLin %A YIN Feng %A LIU Jie %A & LI GanZuo College of Chemistry %A Chemical Engineering %A Liaocheng University %A Liaocheng %A China Key Laboratory of Colloid %A Interface Chemistry %A Ministry of Education %A Sh %A ong University %A Jinan %A China %A
魏西莲 %A 傅式洲 %A 王大奇 %A 孙德志 %A 尹宝霖 %A 尹峰 %A 刘杰 %A 李干佐 %J 科学通报 %D 2009 %I %X The liquid crystalline compound, 2,6-bis(benzylidene)cyclohexanone was synthesized using benzal-dehyde and cyclohexanone as raw materials, and tetrabutyl ammonium bromide as phasetransfer catalyst in the solution of sodium hydroxide. Effect of many factors, such as reaction time, reaction temperature and concentration of sodium hydroxide, was studied. The product was confirmed by IR, 1H-NMR and element analysis. The liquid crystalline behavior of compound was studied by DSC, optical polarizing micrographs a... %K 2 %K 6-二亚苄基环己酮 %K 液晶化合物 %K 织构 %K 流变性能X射线单晶衍射 %U http://www.alljournals.cn/get_abstract_url.aspx?pcid=01BA20E8BA813E1908F3698710BBFEFEE816345F465FEBA5&cid=7C7E63796F062382A606A3A9833B8C05&jid=B40D4BA57FF46E45205A09B4DC283152&aid=B6B89B1E0BDFBC0AD9BF8AF692ACD88D&yid=DE12191FBD62783C&vid=318E4CC20AED4940&iid=94C357A881DFC066&sid=C7461453A367FC85&eid=240CB58995465C01&journal_id=0023-074X&journal_name=科学通报&referenced_num=0&reference_num=0