%0 Journal Article
%T Optimization of ICP-OES for analysis of micro-mass biogenic carbonate<br>微量生物碳酸盐ICP-OES 元素分析中的仪器优化
%A 路 波
%A 于心科
%A 常凤鸣
%A 仇晓华
%A 南青云
%J 海洋科学
%D 2011
%I 
%X To optimize Inductively Coupled Plasma-Optical Emission Spectrometer (ICP-OES) for elemental analysis of micro-mass biogenic carbonate, 1050 groups of instrument parameters, 32 standard solutions with different constituents, 36 analyte pairs and two instrument calibration methods were tested on a Thermo-Fisher iCAP 6300 Radial ICP-OES. The data were analyzed by means of conventional statistics and Scilab. The optimized instrument conditions of Thermo-fisher iCAP 6300 Radial ICP-OES for analysis of Mg/Ca and Sr/Ca ratios in micro-mass biogenic carbonate were enlisted as the follows: glass concentric nebulizer, 0.1 ml/min; coolant gas, default 12 L/min; nebulizer gas pressure, 0.24 MPa; peristaltic pump speed, 16 rpm; radio frequency generator power, 1000 w; view height, 15 mm; analyte lines, Ca 373.690 nm, Mg 279.553 nm {121}, Sr 407.771 nm; instrument calibration method, conventional intensity-concentration method.
%K ICP-OES
%K Scilab
%K Biogenic carbonate
%K Instrument optimization<br>ICP-OES
%K Scilab
%K 生物碳酸盐
%K 仪器优化
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=E62459D214FD64A3C8082E4ED1ABABED5711027BBBDDD35B&cid=2D9C75573FA3E416&jid=DFE7B94EB76B8F26135C9890832CEF6A&aid=2B168B6160CED65F8E996D924D8C2792&yid=9377ED8094509821&vid=6209D9E8050195F5&iid=B31275AF3241DB2D&sid=CA4FD0336C81A37A&eid=DF92D298D3FF1E6E&journal_id=1000-3096&journal_name=海洋科学&referenced_num=0&reference_num=18