%0 Journal Article
%T Synthesis and Characterization of Nickel Nanorods Transferred from Hydrotherally Decomposed Rod-like NiS
%A Yu LUO
%A Jiancheng ZHANG
%A Yue SHEN
%A Shutao JIANG
%A Guoyong LIU
%A <br>Yu
%A LUO
%A Jiancheng
%A ZHANG
%A Yue
%A SHEN
%A Shutao
%A JIANG
%A Guoyong
%A LIU
%J 材料科学技术学报
%D 2007
%I 
%X Powders of hexagonal-structured single-crystalline nickel sulfide nanorods have been synthesized in cetyltrimethyl ammonium bromide (CTAB)/water/hexane/n-pentanol quaternary microemulsion under hydrothermal conditions by using the reaction of carbamide and carbon disulfide as a sulfide source. Single-crystalline nickel nanorods have been synthesized via thermal decomposition by using single-crystalline nickel sulfide nanorods as precursor. The influence of different reaction parameters on the morphology of the products has been investigated. The structure, morphology and magnetic properties of the products were characterized by X-ray diffraction (XRD), transmission electron microscope (TEM), thermogravimetric analysis-differential scanning calorimeter (TGA-DSC) and vibrating sample magnetometer (VSM). The results of magnetic measurements showed that the specific saturation magnetization (σs) and coercivity values (Hc) of nickel nanorods were 37.5 emu/g and 68.5 Oe, respectively.
%K Hydrothermal microemulsion
%K Nickel sulfide nanorods
%K Nickel nanorods
%K Magnetic properties<br>镍元素
%K 硫化物
%K 磁性材料
%K 微型乳剂
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=5B3AB970F71A803DEACDC0559115BFCF0A068CD97DD29835&cid=84529CA2B2E519AC&jid=324DC3CAB22330DB19158AE0A9B7BFA5&aid=F1839B40C8AE1F67DADAC765731D7F92&yid=A732AF04DDA03BB3&vid=EA389574707BDED3&iid=94C357A881DFC066&sid=D5970ECA7D10A7B1&eid=C7461453A367FC85&journal_id=1005-0302&journal_name=材料科学技术学报&referenced_num=0&reference_num=26