%0 Journal Article
%T Influence of Ethylene Glycol on the Formation of Calcium Phosphate Nanocrystals
%A Yi ZUO
%A Yubao LI
%A Jie WEI
%A Yonggang YAN
%A
YiZUO
%A YubaoLI
%A JieWEI
%A YonggangYAN
%J 材料科学技术学报
%D 2003
%I
%X A synthesis route of using calcium hydroxide Ca(OH)2 with ethylene glycol solvent and orthophosphoric acid (H3PO4) as reagents is described. Three ratios of ethylene glycol to distilled water 1:0, 1:1 and 0:1 are used as diluting media for Ca(OH)2. Crystals of different morphology and composition are formed under weak alkaline circumstance at pH 7.0-8.0. Acicular calcium phosphate nanocrystals are prepared in pure ethylene glycol while rod-like calcium phosphate nanocrystals form in pure distilled water. The nanograde size of the former is smaller than that of the latter. Calcium-deficient apatite (CDAP) is obtained with a Ca/P molar ratio of 1.66. Therefore, it was deduced that the usage of ethylene glycol solvent could influence the formation of calcium phosphate crystal lattice.
%K Acicular nanocrystals
%K Calcium phosphate
%K Ethylene glycol solvent
%K Weak alkaline circumstance
乙烯
%K 乙二醇
%K 磷酸钙
%K 纳米晶体材料
%K 氢氧化钙
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=5B3AB970F71A803DEACDC0559115BFCF0A068CD97DD29835&cid=84529CA2B2E519AC&jid=324DC3CAB22330DB19158AE0A9B7BFA5&aid=D25AC06D6C751473&yid=D43C4A19B2EE3C0A&vid=2A8D03AD8076A2E3&iid=B31275AF3241DB2D&sid=3EABEBD973E45554&eid=039DCCB9394D9766&journal_id=1005-0302&journal_name=材料科学技术学报&referenced_num=0&reference_num=33