%0 Journal Article %T DOPING AND MICROSTRUCTURE OF NANOCRYSTALLINE SnO_2
二氧化锡纳米粉掺杂及其显微结构 %A WANG YuanSheng %A YANG Yumin %A HUANG Zhaoxin %A
王元生 %A 杨裕民 %A 黄兆新 %J 材料研究学报 %D 1998 %I %X SnO2 nanocrystalline powder doped with variable ratios of Fe have been preparedty sol-gel method. The phase and grain-size, and their evolution of the powder have been studied by XRD, TEM, DTA and Mossbauer spectrometer. For the pewder with Fe/Sn atomic ratios range from 14.3/100 to 38-5/100, they are all SnO2 phases with Fe atoms as the solute in the lattice. Thegrain-size reaches about 2nm. Fe doping takes the role of reducing SnO2 grain-size, and restrain the grain growth during heat treatment, and thus favorable to keep the nanostructure of the material whenthe powder be sintered to form the gas-sensitive elements. %K nanocrystalline %K doping %K grain-size
纳米材料 %K 掺杂 %K 晶粒度 %K 二氧化锡 %K 显微结构 %U http://www.alljournals.cn/get_abstract_url.aspx?pcid=5B3AB970F71A803DEACDC0559115BFCF0A068CD97DD29835&cid=84529CA2B2E519AC&jid=C101C4C04993B4D94FCD8446E6CBEB3B&aid=AA7391F1DCBFAE69&yid=8CAA3A429E3EA654&vid=59906B3B2830C2C5&iid=94C357A881DFC066&sid=20ADD38F841C6A4B&eid=D45762219109E903&journal_id=1005-3093&journal_name=材料研究学报&referenced_num=10&reference_num=7