%0 Journal Article %T Three-Step Growth Optimization of AlN Epilayers by MOCVD
%A PENG Ming-Zeng %A GUO Li-Wei %A ZHANG Jie %A YU Nai-Sen %A ZHU Xue-Liang %A YANJian-Feng %A GE Bin-Hui %A JIA Hai-Qiang %A CHEN Hong %A ZHOU Jun-Ming %A
%J 中国物理快报 %D 2008 %I %X A three-step growth process is developed for depositing high-quality aluminium-nitride (AlN) epilayers on (001) sapphire by low pressure metalorganic chemical vapour deposition (LP-MOCVD). We adopt a low temperature (LT) AlN nucleation layer (NL), and two high temperature (HT) AlN layers with different V/III ratios. Our results reveal that the optimal NL temperature is 840--880°C, and there exists a proper growth switching from low to high V/III ratio for further reducing threading dislocations (TDs). The screw-type TD density of the optimized AlN film is just 7.86×106cm-2, aboutthree orders lower than its edge-type one of 2×109cm-2 estimated by high-resolution x-ray diffraction (HRXRD) and cross-sectional transmission electronmicroscopy (TEM). %K 81 %K 05 %K Ea %K 81 %K 15 %K Gh %K 61 %K 10 %K -i %K 68 %K 37 %K Lp
%U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=47EA7CFDDEBB28E0&jid=E27DA92E19FE279A273627875A70D74D&aid=53CD15EE2D7DC18A91FE48EDE4A91696&yid=67289AFF6305E306&vid=C5154311167311FE&iid=B31275AF3241DB2D&sid=D53D369D01F50334&eid=3A9DC0CD8A6F1E57&journal_id=0256-307X&journal_name=中国物理快报&referenced_num=0&reference_num=0