%0 Journal Article %T Preparation of Zinc Sulfide Nano-particles by High-Gravity Method
超重力法制备纳米硫化锌 %A LI Ya-Ling %A WANG Yu-Hong %A CHEN Jian-Feng %A Jimmy Yun %A
李亚玲 %A 王玉红 %A 陈建峰 %A 甄崇礼 %J 无机材料学报 %D 2003 %I Science Press %X By using zinc nitrate and hydrogen sulfide as source materials, nanometer zinc sulfide was synthesized by a high gravity method in a rotating packed bed. The effect of aging time on product sizes was investigated and 48h was chosen. Well-dispersed nanometer zinc sulfide particles with a sphalerite crystal phase were prepared. The crystal structure, optical properties, size and morphology of the product were also characterized by XRD, UV-Vis spectrophotometer and TEM. The results show that the average particle size of ZnS obtained is about 30nm and the conversion rate is 97.5 percent. %K high gravity %K rotating packed bed %K nano-ZnS %K preparation
超重力旋转床 %K 纳米硫化锌 %K 制备 %U http://www.alljournals.cn/get_abstract_url.aspx?pcid=5B3AB970F71A803DEACDC0559115BFCF0A068CD97DD29835&cid=84529CA2B2E519AC&jid=ABC0063016AF57E1C73EF43C8D2212BD&aid=1B112C124AA28711&yid=D43C4A19B2EE3C0A&vid=13553B2D12F347E8&iid=B31275AF3241DB2D&sid=6300C37F864D5DEA&eid=29BFCA84676506CC&journal_id=1000-324X&journal_name=无机材料学报&referenced_num=7&reference_num=4