%0 Journal Article %T Charaterization of Graphitization Degree of C/C Composites by Laser Raman Microspectroscopy
C/C复合材料石墨化度的喇曼光谱表征 %A ZHANG Fu-Qin %A HUANG Qi-Zhong %A HUANG Bai-Yun %A GONG Qian-Ming %A CHEN Teng-Fei %A XIONG Xiang %A
张福勤 %A 黄启忠 %A 黄伯云 %A 巩前明 %A 陈腾飞 %A 熊翔 %J 无机材料学报 %D 2003 %I Science Press %X The structural parameters of carbon fiber, pitch-derived carbon and pyrolytic carbon in C/C composites were charaterized by laser Raman microspectroscopy and XRD. In Raman spectra of these carbons, two bands named D and G were observed near 1336.73cm-1 and 1581.00cm-1 respectively, the peak positions do not but the relative intensities of the two bands change with heat treatment temperatures. The relationship between the XRD data of graphitization degree g and R-1 where R is the relative intensity of band D to band G was plotted, the result shows that g increases with the increase of R-1, but the gradient of the R-1-g curve decreases and gradually tends to zero with the increase of R-1, and their relation can be written into the following equation: g = 1- e-2-H(1/R-0.34). The foundation of the correlation between R-1 and g makes it possible to analyze the local distribution of graphitization degree in C/C composites. %K C/C composite %K graphitization degree %K laser Raman microspectroscopy %K XRD
C/C复合材料 %K 石墨化度 %K 显微激光喇曼光谱 %K XRD %U http://www.alljournals.cn/get_abstract_url.aspx?pcid=5B3AB970F71A803DEACDC0559115BFCF0A068CD97DD29835&cid=84529CA2B2E519AC&jid=ABC0063016AF57E1C73EF43C8D2212BD&aid=A61EE317F74E549D&yid=D43C4A19B2EE3C0A&vid=13553B2D12F347E8&iid=0B39A22176CE99FB&sid=3E3EF0DB5E6F2DA9&eid=2E41258BCB9A7DB2&journal_id=1000-324X&journal_name=无机材料学报&referenced_num=7&reference_num=10