%0 Journal Article %T Pore structure determination of mesoporous SiO2 thin films by slow positron annihilation spectroscopy
介孔SiO2薄膜孔结构的慢正电子技术表征 %A Wang Qiao-Zhan %A Yu Run-Sheng %A Qin Xiu-Bo %A Li Yu-Xiao %A Wang Bao-Yi %A Jia Quan-Jie %A
王巧占 %A 于润升 %A 秦秀波 %A 李玉晓 %A 王宝义 %A 贾全杰 %J 物理学报 %D 2009 %I %X Mesoporous silica thin films with different pore shapes were prepared by evaporation induced self-assembly method. The synchrotron radiation x-ray reflectivity and slow positron annihilation techniques were used to characterize the pore structures. The results indicated that with increase of the spin-coating speed, the pore structure transformed from 3-D cubic to 2-D hexagonal, the average porosity also decreased. The correlation of the film structures and positron annihilation parameters was songht for with FT-IR spectroscopy and isotropic inorganic pore contraction model. %K synchrotron radiation %K x-ray reflectivity %K Doppler broadening %K positronium time-of-flight
同步辐射, %K X射线反射率, %K Doppler展宽, %K 正电子素飞行时间谱 %U http://www.alljournals.cn/get_abstract_url.aspx?pcid=6E709DC38FA1D09A4B578DD0906875B5B44D4D294832BB8E&cid=47EA7CFDDEBB28E0&jid=29DF2CB55EF687E7EFA80DFD4B978260&aid=88ABEA1C5D54BC2BF5B19B44855E4950&yid=DE12191FBD62783C&vid=9FFCC7AF50CAEBF7&iid=59906B3B2830C2C5&sid=4F4FB6601BA924E8&eid=33026C7412CAA2B5&journal_id=1000-3290&journal_name=物理学报&referenced_num=0&reference_num=0