%0 Journal Article
%T Evaluation of Volatile Compounds of ˇ°Tiger Nut Beverageˇ± (Orxata de Xufla) Headspace by Optimized Solid-Phase Micro-Extraction
%A Bruna Klein
%A Joan-Josep Gallardo-Chac¨®n
%A Idoia Codina-Torrella
%A Antonio-Jos¨¦ Trujillo
%A Bibiana Juan
%J Open Access Library Journal
%V 1
%N 8
%P 1-15
%@ 2333-9721
%D 2014
%I Open Access Library
%R 10.4236/oalib.1101015
%X The aroma profile of ˇ°tiger nut beverageˇ± (orxata de
xufla) was investigated by headspace solid- phase micro-extraction (HS-SPME)
combined with gas chromatography-mass spectrometry (GC- MS). Polidimethilsiloxane/divinylbenzene
(PDMS/DVB), carboxen/polydimethylsiloxane (CAR/ PDMS), polyacrylate (PA) and
divinylbenzene/carboxen/polydimethylsiloxane (DVB/CAR/PDMS) fibers were tested
and compared for sensitivity beyond conditions that might affect the SPME
procedure, such as temperature, concentration of ions and sample volume. The
SPME fiber coated with DVB/CAR/PDMS presented the most efficient extraction
compounds from the headspace of the product, particularly when the volatiles
were extracted at 60ˇć with 2 mL of the sample volume. The addition of salt did
not show any significant advantage for the qualification of the volatile
fraction. Eighty-three compounds were identified or tentatively identified by
GC-MS, being terpenes the most abundant group.
%K Headspace Solid-Phase Micro-Extraction (SPME)
%K Gas Chromatography-Mass Spectrometry (GC-MS)
%K Tiger Nut Beverage
%K Volatile Compounds
%U http://www.oalib.com/paper/3125393